By Kurt Busiek, Ben Abernathy
Every thing you want to learn about Astro urban and its many particular areas and faces: local courses, eating place strategies, highlights, neighborhood pursuits, advertisements for neighborhood companies, a historical past of the town, a map or even a consultant to the who’s-who of the hero elite illustrated by way of fan-favorite artists.
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Additional resources for Astro City - A Visitor's Guide
Ketoesters\ are reduced with higher levels of enantio! called Mar! diols ð60CJC1475Ł[ The acid! isomer ð78CC0318Ł as predicted by theoretical studies ð73T1146Ł[ Mes! borabicyclo! diboranes upon reaction with diborane[ These diboranes are con! verted to primary alcohols upon usual peroxidative workup "Scheme 1# ð56JA180Ł[ BR2 2 BH3 H2O2 NaOH BR2 BR2 OH Scheme 2 1[91[0[1[0 Stereo! pinene is a good example of the regio! based Functional Groups seen in such reactions^ the initial product of addition is diisopinocampheylborane "Ipc1BH#\ arising from regio!
Bination with either I1:CuO = HBF3 ð76CC0380\ 89JCS"P0#1796Ł or the stable solid reagent bis"pyr! transfer catalysts ð71TL3540\ 78JCR"S#093\ 81JCS"P0#1298Ł[ Alter! 90Ł[ 1[90[3[3 Alkyl Bromides from Alcohols and their Derivatives A number of methods for the conversion of alcohols to halides "including bromides# have already been discussed in Section 1[90[0[3[0[ As is the case with the other halides\ conversion of alcohols to alkyl bromides using HBr works well "particularly in systems where the SN0 pathway is facilitated by stabilisation of the intermediate carbocation ð30OSC"0#14\ 76JOC4459Ł\ but rearrangements of the carbonium ion sometimes occur[ While the use of phase transfer catalysis can reduce rearrangements considerably ð76TL0112Ł\ and has even facilitated the preparation of primary bromides using HBr ð76JCS"P0#1046Ł\ a far more popular reagent\ which also leads to less rearrangement\ is phosphorus tribromide\ PBr2[ Although PBr2 can be generated in situ from phosphorus and bromine ð30OSC"0#25\ 32OSC"1#297Ł\ it is more common to use commercially available liquid PBr2 ð32OSC"1#247Ł[ The presence of pyridine can help ð44OSC"2#682Ł\ or the PBr2 can be conveniently adsorbed onto a resin!
Selective ð81TL5396Ł and has been used to synthesise all four isomers of disparlure ð81TL5300Ł[ To accomplish highly selective hydroxylation of a\b! unsaturated amides\ a modi_ed AD! mix employing a _vefold increase in the ligand and potassium osmate is required ð82TL1968Ł[ When this new\ improved mix was used\ both a\b!
Astro City - A Visitor's Guide by Kurt Busiek, Ben Abernathy